Micro-determination of mercury by cold vapor atomic absorption utilizing double-beam spectrophotometer.

Determination of mercury in the urine by atomic absorption spectrometry - cold vapor technique

Urine is a liquid waste product of the body. Substances that are ingested and fail to be apsorbed are excreted, solid waste through the intestines, the urine through the kidney and ureter and another fluid from the body through perspiration. Determination of mercury content of urine is not included in routine examinations, but mercury can be present in urine at concentrations that could have se...

Modified determination of total and inorganic mercury in urine by cold vapor atomic absorption sectrometry.

In this procedure a single-beam spectrophotometer is used without background correction. By the method of Magos [Analyst (London) 96, 847 (1971)] mercury in undigested urine is complexed to L-cysteine in acid solution. At high pH and in the presence of stannous ions, mercury ions are reduced to elemental mercury. The mercury vapor is partitioned above the reagent solution in a specially designe...

Use of Different Gold Amalgamation Techniques in Mercury Determination by Cold Vapor Atomic Absorption Spectrometry

Determination of mercury(II) ion by electrochemical cold vapor generation atomic absorption spectrometry.

A technique for determination of mercury is described; it is based on electrolytic reduction of Hg(II) ion on a graphite cathode, the trapping of mercury vapor and its volatilization into a quartz tube aligned in the optical path of an atomic absorption spectrometer. The electrochemical cell consisted of a graphite cathode and an anode operating with constant direct current for the production o...

A sequential injection cold-vapor atomic absorption method for the determination of total mercury.

A sequential injection (SI) method for the determination of mercury via cold vapor atomic absorption spectrophotometry is presented. The method differs from flow injection (FI) cold vapor methods for the determination of mercury because of the simplicity of the system required for the method: one pump, one valve, a gas-liquid separator, and an atomic absorption spectrophotometer equipped with a...